首页 >> >>ҵ̬ >> ЧҺɫ׷ⶨ͹ʲиʲĺ
详细内容

ЧҺɫ׷ⶨ͹ʲиʲĺ

    ժҪʲΪֲʲݡ͹ʲݻʲݵĸ书ܲƢֹȡֹʹȽⶾҩԡҪиʲἰʲɷ֣иʲΪִҩӦо֤ʵпάסͱνⶾǿ߹ܵá

      ĿǰԸʲݵƣҪΧƸʲɷֽжԡһļ顣2005桶йҩ䡷RP-HPLCԪȶϴѷⶨʲķ涨ʲẬõ2%ۣݡʵ2005桶йҩ䡷һʲẬⶨ¼VID²ߣRP-HPLCⶨʲĺ㡢٣Ժãȶڸʲļרǿ1Լ1.1Agilend1100ϵҺɫǡԪáDADѧվ1200Զ

      1.2ԼʲᵥΣmonoam0niumglycyrrhitinateƷйҩƷƷ춨ʲݣglycyrrhizainflatabatƷ½ҽҩɷ޹˾״ɫ״泥ᣨˮ˫ˮ

      2ʵ鷽2.1ɫZORBAXExundC184.6mm250mm5mΪ̶ࣻ״-0.2mol/LҺ-ᣨ67331ΪࣻⲨ250nm1mlmin-1Ϊ¡ЧԸʲƣӦ2000ɷ7minڼɳ꣬ԪȶϴȫΪ020min¼ɫͼͼ12

      2.2ƷҺƱܳȡ80صĸʲᵥ0.1gƷ100mlƿУˮܽⲢϡ̶ȣҡȣʹÿmlиʲᵥ1mgƷҺ

      2.3ƷҺƱȡʲݣϸ3ɸú80أܳȡ0.3g100mlƿУԼ45ml250WƵ20KH230minȡ䣬̶ȣҡȣ΢Ĥ0.45m˹ȡҺΪƷҺ

      2.4ⶨȡƷҺƷҺ10lעҺɫǣ¼ɫͼԶƷҺɫͼиʲķ3ƽ귨ʲиʲĺ%W/W

      2.5ԹϵȡƷҺ1.02.04.08.010.0ml100mlƿУˮϡ̶ȣҡȣֱ10l¼ԽgΪ꣨XAΪ꣨YƱ׼ߡʲع鷽ΪY=3.00029X 1.23099r=0.99989ԷΧ0.10331.0330g

      2.6ܶ龫ȡƷҺɫ½10lظ5ΣԱɷֱַ㣬ʲRSD=1.21%

      2.7ȶ龫ȡƷҺ10lֱ02468h¼ʲRSD=1.45%n=5

      2.8ȡͬһθʲҩİ2.3ȡƱ5ݹҺֱȡ10l¼ʲRSD=1.32%

      2.9ʲⶨȡ֪ĸʲƷĩԼ0.2gܳƶ9ݣ10mlƿУ1mg/mlʲƷҺ1ml2.3²10l2.4ⶨ¼ʣʲƽΪ99.04%RSD=0.79%11ʲʵԣ

      2.10Ʒⶨȡ6Ʒ2.3ȡƱ2.4ⶨظⶨ3ΣҩʲݵƽΪ7.85%RSD=0.85%

      33.1ϴܼϵͳѡʵΪRP-HPLCԪȶϴѷѡ״-0.2mol/LҺ-ᣨ67331ΪϴܼǻڸʲԪȶϴϵͳӦԵĿ͹ʲкиʲᡢʲյȳɷֻ֣Ҫѡ˵ϴܼϵͳԴʹֵķϵϴ󣬴ﵽ߷Чʵ֤÷򵥡У豸ҪݶϴΪͣһ豸ڼ⣬ҿǿרص㡣

      3.2ڸʲҩʲȡĸʲᣬ֮ͨȻʲᣬȻʲ˳칹˳ʽʲẬΪߣʽʲẬ͡ʵδܽʾ칹߷룬칹廯ѧṹֻ͹ʲݱδзʽʲйأдһо

下一篇ҩᰬ˾̪Ƭ
技术支持 ȫ | 管理登录